Contact Info
Stuart Chalk, Ph.D.
Department of Chemistry
University of North Florida
Phone: 1-904-620-1938
Fax: 1-904-620-3535
Email: schalk@unf.edu
Website: @unf
Spectrophotometry
Citations 2
"Design And Performance Of A New Continuous-flow Sample-introduction System For Flame Infrared-emission Spectrometry: Applications In Process Analysis, Flow Injection Analysis, And Ion-exchange High Performance Liquid Chromatography"
Talanta
1993 Volume 40, Issue 6 Pages 867-878
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Abstract:
The cited system involves a specially designed purge cell to strip dissolved CO2 from solution into a H gas stream that serves as fuel for the hydrogen/air flame of the flame IR-emission (FIRE) radiometer. Sample stream is fed into the top of the cell through a PTFE tube and the H purge gas is supplied through a gas dispersion tube at the bottom of the cell. A side-arm links the cell to the FIRE burner and the spent analytical solution drains away through a bottom outlet. The system was applied in the process and FIA modes to the determination of total inorganic C in tap-water. In both modes the sample was mixed with 0.25 M HCl to release CO2. The procedure was extended to the determination of non-volatile organic materials by oxidizing the analytes to dissolved CO2 with peroxydisulfate in the presence of a Ag+ catalyst before purging. No details of detection limits or RSD are given.
Carbon, total
Water
'Hyphenated Flow Injection Systems And High Discrimination Instruments', Talanta, 1995 42(2) 151-169
"Hyphenated Flow Injection Systems And High Discrimination Instruments"
Talanta
1995 Volume 42, Issue 2 Pages 151-169
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Abstract:
A review is presented of state-of-the-art FIA coupled to instruments capable of providing multidetection and/or multi-information. Tables are presented of the methods of FIA coupled with ICP-AES, ICP-MS, FTIR, MS, MECA, NMR and flame IR emission spectrometry with references. Interfaces, sample introduction, sample handling, online separation processes and speciation studies are discussed. (190 references).
Detector
Interface
Review
Speciation