FAD: Techniques

Contact Info

Stuart Chalk, Ph.D.
Department of Chemistry
University of North Florida
Phone: 1-904-620-1938
Fax: 1-904-620-3535
Email: schalk@unf.edu
Website: @unf

Polarography

Classification: Polarography -> hydrodynamic

Citations 1

'Voltammetric Detector For Flowing Systems', Z. Chem., 1988 28(3) 113-114

"Voltammetric Detector For Flowing Systems"
Z. Chem. 1988 Volume 28, Issue 3 Pages 113-114

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Gabriele Jokuszies, Hendrik Emons

Abstract: A wall-jet cell comprising a Pt working electrode, a Ag counter electrode and a Ag - AgCl reference electrode (described and illustrated) was incorporated into a detector for HPLC or flow injection analysis. The detector cell was characterized by the amperometric oxidation of K4Fe(CN)6. The most favourable working electrode potential, determined by recording hydrodynamic polarograms of 1 mM K4Fe(CN)6 in 0.1 M KCl at increasing electrode potential from 0 to +1 V, was +0.4 V.

Apparatus Detector