Contact Info
Stuart Chalk, Ph.D.
Department of Chemistry
University of North Florida
Phone: 1-904-620-1938
Fax: 1-904-620-3535
Email: schalk@unf.edu
Website: @unf
Electroluminescence
Classification:
Electroluminescence
Citations 1
"Development And Characterization Of Anodically Initiated Luminescent Detection For Alcohols And Carbohydrates"
Anal. Chim. Acta
1997 Volume 337, Issue 2 Pages 207-215
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4260-EP2377845A1, 4260-EP2377849A2, 4260-EP2380874A2, InChI=1/C2H6O/c1-2-3/h3H,2H2,1H, 28147-EP2277868A1, 28147-EP2277869A1, 28147-EP2277870A1, 28147-EP2295422A2, 28147-EP2298305A1, 28147-EP2298769A1, 28147-EP2308852A1, 28147-EP2308878A2, 28147-EP2313400A1, 28147-EP2371823A1, 48516-EP2311824A1, 48516-EP2311828A1, 48516-EP2380568A1, 3B4-0664, Anti-EphB1 (ELK Receptor)-CY antibody produced in sheep, 1E37B0D2-6209-4B03-A57D-500F3223C2DA, 68475-56-9', 'total' => '15', 'inchi' => 'InChI=1S/C2H6O/c1-2-3/h3H,2H2,1H3', 'inchikey' => 'LFQSCWFLJHTTHZ-UHFFFAOYSA-N', 'formula' => 'C2H6O', 'oxstate' => 'Zero', 'url' => '', 'charge' => '0', 'class1' => '', 'class2' => '', 'class3' => '', 'class4' => '', 'class5' => '', 'isgroup' => 'no', 'checked' => 'no', 'citation_count' => '0', 'updated' => '2015-12-11 16:18:02', 'first' => 'A', 'nametotal' => 'Alcohols**15', 'AnalytesCitation' => array( [maximum depth reached] ) ), (int) 1 => array( 'id' => '00508', 'name' => 'Carbohydrates', 'iupac_name' => '', 'casrn' => 'NA', 'synonyms' => 'NA', 'total' => '46', 'inchi' => '', 'inchikey' => '', 'formula' => '', 'oxstate' => null, 'url' => '', 'charge' => null, 'class1' => 'Organic compound', 'class2' => 'NA', 'class3' => 'NA', 'class4' => 'Molecule', 'class5' => 'NA', 'isgroup' => 'yes', 'checked' => 'yes', 'citation_count' => '0', 'updated' => '2015-12-11 09:54:00', 'first' => 'C', 'nametotal' => 'Carbohydrates**46', 'AnalytesCitation' => array( [maximum depth reached] ) ) ), 'Matrix' => array(), 'Keyword' => array() ) $i = (int) 0 $path = '' $a = '' $url = 'http://dx.doi.org/10.1016/S0003-2670(96)00399-6' $aus = 'Hajime Karatani*, Motohiro Kojima, Hiroyoshi Minakuchi, Naohiro Soga and Takahiro Shizuki'include - APP/View/Elements/citation.ctp, line 40 View::_evaluate() - CORE/Cake/View/View.php, line 971 View::_render() - CORE/Cake/View/View.php, line 933 View::_renderElement() - CORE/Cake/View/View.php, line 1224 View::element() - CORE/Cake/View/View.php, line 418 include - APP/View/Techniques/view.ctp, line 52 View::_evaluate() - CORE/Cake/View/View.php, line 971 View::_render() - CORE/Cake/View/View.php, line 933 View::render() - CORE/Cake/View/View.php, line 473 Controller::render() - CORE/Cake/Controller/Controller.php, line 968 Dispatcher::_invoke() - CORE/Cake/Routing/Dispatcher.php, line 200 Dispatcher::dispatch() - CORE/Cake/Routing/Dispatcher.php, line 167 [main] - APP/webroot/index.php, line 109
Abstract:
A detection method for hydroxyl compounds such as alcohols and carbohydrates was developed based on luminescence initiated by electro-oxidation at a vitreous C electrode in alkaline aqueous solutions. The method was employed in a FIA system. Sample volumes of 50 µL were injected into a 1 M NaOH carrier stream (5 ml/min) containing 50 µM-fluorescein (to enhance signal) and propelled through a detection cell (30 µL volume) equipped with a vitreous C working electrode maintained at 1.3 V vs. Ag/AgCl reference electrode (Pt auxiliary electrode). The luminescence intensity was detected with a photomultiplier tube. Linear calibration graphs were obtained for 10 µM to 1 mM of various carbohydrate and simple hydroxyl compounds by the double logarithmic plotting of peak luminescence intensity vs. concentration. The detection limits were 0.3-13.5 µM.
Alcohols
Carbohydrates