"Indirect Potentiometric Flow Injection Determination Of Silver In Photographic Fixing Solutions"
Anal. Chim. Acta
1989 Volume 220, Issue 1 Pages 287-291
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Frazier Nyasulu
Abstract:
Sample (0.4 ml) is injected into a stream of water that merges with a stream of 2 M H2SO4 at 70°C, and the SO2 produced is removed by diffusion through a 75-cm coil of Gore-Tex microporous PTFE tubing (pore size 3.5 µm). An excess of S2- in 6 M NaOH is added downstream of the coil, and the decrease in S2- concentration. is measured with a Ag - Ag2S electrode. The calibration graph is rectilinear from 1 mg L-1 to 10 g L-1 of Ag, and the detection limit is 0.04 mg l-1. Results for five fixing solution agreed well with those obtained by AAS.
Silver
Fixing solution
Diffusion
Microporous membrane
Goretex
Method comparison
Indirect
