"Flow Injection Analysis As A Tool For Studying Polymer Modified Electrodes"
Anal. Chim. Acta
1996 Volume 329, Issue 1 Pages 181-189
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Wladyslaw W. Kubiak*, and Joseph Wang
Abstract:
A FIA system was described for studying the permeation, selectivity and dynamic properties of polymer films deposited on a glassy C disc electrode. The FIA system was equipped with a 500 µL injection loop and a thin-layer amperometric detector fitted with two glassy C electrodes (3 mm diameter), a Ag/AgCl (3 M NaCl) reference electrode and a steel auxiliary electrode. One of the glassy C electrodes was coated a polymer film, e.g., cellulose acetate, Nafion, polypyrrole, polyaniline or polyvinylpyridine. Several different test substances were injected into a 0.1 M phosphate buffer carrier stream of pH 7.4 and the responses obtained from the coated and uncoated working electrodes were compared. The advantages of the flow injection manifold are discussed; equations are derived to support the discussion.
Detector
