University of North Florida
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Stuart Chalk, Ph.D.
Department of Chemistry
University of North Florida
Phone: 1-904-620-1938
Fax: 1-904-620-3535
Email: schalk@unf.edu
Website: @unf

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NRCC MESS-1

Classification: Reference Material -> NRCC -> MESS-1 -> Marine sediment

Citations 1

"A Flow Injection/hydride Generation System For The Determination Of Arsenic By Inductively-coupled Plasma Atomic Emission Spectrometry"
Anal. Chim. Acta 1984 Volume 161, Issue 1 Pages 275-283
R. R. Liversage and J. C. Van Loon, J. C. De Andrade

Abstract: After optimizing the concentration. of HCl and NaI in the test solution, the concentration. of NaBH4, sample and reductant volume and flow rate, Ar carrier-gas flow rate and r.f. power, As (10 to 1000 ppb) was determined in NBS orchard leaves, coal fly ash and river sediment and NRCC MESS-1 and BCSS-1 standard reference materials with good accuracy and precision by using an ARL 34000 Quantometer. The coefficient of variation (n = 10) at the 100-ppb level of As was 7.2%, and the detection limit was 1.4 ng for a 0.17 mL sample volume The calibration graph was rectilinear for 0.01 to 1 ppm of As. Cobalt, Ni, Ag, Au, Bi, Te and Sn interfered. About 200 injections h-1 were possible.
Arsenic Spectrophotometry Interferences Reference material