University of North Florida
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Stuart Chalk, Ph.D.
Department of Chemistry
University of North Florida
Phone: 1-904-620-1938
Fax: 1-904-620-3535
Email: schalk@unf.edu
Website: @unf

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BCR 97

Classification: Reference Material -> BCR -> 97 -> Iron

Citations 1

"Determination Of Trace Elements In Unalloyed Steels By Flow Injection Inductively Coupled Plasma Mass Spectrometry"
J. Anal. At. Spectrom. 1995 Volume 10, Issue 6 Pages 449-453
Aurora G. Coedo and Teresa Dorado

Abstract: Steel (250 mg) was treated with 7 mL 65% HNO3, 200 µL 40% HF and 3 mL water and the mixture was digested in a microwave oven (program details given). The oven was cooled, the contents were transferred to a calibrated flask and 2.5 µg each of Be, Tl and Rh (internal standards) were added. The solution was diluted to 50 mL with 1% HNO3 and a 250 µL portion of the solution was pumped into the nebulizer (2.8 ml/min), mixed with the nebulizer gas (1.1 ml/min) and analyzed by ICP-MS (operating conditions given). The RSD was 3% for all analytes at concentrations 1 µg/g. The method was applied to the analysis of two pure Fe reference materials (BCR CRM 097 and NIST SRM 365). Results agreed well with certified values.
Trace elements Mass spectrometry Sample preparation Internal standard Reference material