University of North Florida
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Stuart Chalk, Ph.D.
Department of Chemistry
University of North Florida
Phone: 1-904-620-1938
Fax: 1-904-620-3535
Email: schalk@unf.edu
Website: @unf

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Proceedings of the Analytical Division of the Chemical Society

  • Publisher: Royal Society of Chemistry
  • FAD Code: PADC
  • CODEN: ANCOFE
  • ISSN: 0144-557X
  • Abbreviation: Proc. Anal. Div. Chem. Soc.
  • DOI Prefix: 10.1039
  • Other Name(s): Proceedings of the Society for Analytical Chemistry (From 1964 v1-8),Proceedings of the Analytical Division of the RSC (as of 1972 v9-11),Proceedings of the Analytical Division of the Chemical Society (as of 1975 v12-18),Analytical Proceedings (as of 1980
  • Language: English
  • Comments: Fulltext from 1975 V12

Citations 3

"Flow Jnection Technqiues. Monitoring Chemiluminescent Reactions By Flow Injection Analysis"
Proc. Anal. Div. Chem. Soc. 1979 Volume 16, Issue 9 Pages 262-264
J. L. Burguera and Alan Townshend

Abstract: The performance of an app. for monitoring chemiluminescent reactions by flow injection analysis was described using the chemiluminescence that occurs when Et3N is oxidized by BzOOH in Me2CO and the Co-catalyzed oxidation of luminol as examples. Efficient mixing and not too rapid removal of analyte from the cell are necessary. Thus the detection limits were 2.5 µg Et3N/0.5 mL sample and 10^-6 ppm Co.
Triethylamine Cobalt Bioluminescence Chemiluminescence Apparatus Indirect Catalysis

"Studies In Flow Injection Analysis"
Proc. Anal. Div. Chem. Soc. 1979 Volume 16, Issue 1 Pages 4-7
B. Fields, L. Dajer de Torrijos, E. J. Greenhow, Aileen M. Prescott, Michael Cooke, Samuel J. Lyle, Saber Tehrani, P. J. Barlow, D. R. Crump, A. K. Khera, D. G. Wibberley, D. S. Macintyre, B. G. Cooksey, J. M. Ottaway, J. F. Alder, R. M. Bombelka and G. F

Abstract: The application of flow injection analysis to the simultaneous spectrophotometric determination of two metals in a sample is described and a novel phototransducer which improved peak detection is discussed. Thus, an aqueous HCl sample containing Pb(II) and V(V) at pH 2 was injected into a stream 10^-3 M in 4-(2-pyridylazo)resorcinol (I) buffered in NH3 at pH 9.9. The changes with time in the peaks owing to the V-I complex, formed at pH 2, and the Pb-I complex, formed at pH 9, were observed Pb was determined with 1-2% relative standard deviation in the presence of varying amounts of V but V could be determined with only limited precision in the presence of a constant amt. of Pb. The use of refractometry to measure peaks in flow injection analysis was also discussed with reference to some examples with aqueous NaCl. With the phototransducer, 100 ppb Co(II) could be detected with a relative standard deviation of ~1%.
Lead(2+) Vanadium(V) Cobalt(II) Refractometry Spectrophotometry Simultaneous analysis Refractive index Photoelectric devices pH