Contact Info
Stuart Chalk, Ph.D.
Department of Chemistry
University of North Florida
Phone: 1-904-620-1938
Fax: 1-904-620-3535
Email: schalk@unf.edu
Website: @unf
Vanillic acid
- IUPAC Name: 4-hydroxy-3-methoxybenzoic acid
- Molecular Formula: C8H8O4
- CAS Registry Number: 121-34-6
- InChI: InChI=1S/C8H8O4/c1-12-7-4-5(8(10)11)2-3-6(7)9/h2-4,9H,1H3,(H,10,11)
- InChI Key: WKOLLVMJNQIZCI-UHFFFAOYSA-N
Citations 1
"Selective Flow-rate-independent Flow Injection Analysis Technique: Combination Of A Single-bead String Reactor With Rapid-scan Square-wave Voltammetry"
Anal. Sci.
1989 Volume 5, Issue 5 Pages 567-570
D. YOSHIZAWA, K. SHIMIZU, G. P. SATO, K. KUMAKURA and K. AOKI
Abstract:
The response dependence of the flow injection system on the flow rate was minimized by use of a single-bead string reactor. The reactor tube consisted of PTFE tubing (1 m x 0.7 mm) packed with glass beads of diameter slightly smaller than that of the tubing. The system was equipped with an electrochemical detector incorporating two circular vitreous-carbon working electrodes and a Ag - AgCl reference electrode; voltammograms that were independent of flow rate were obtained by means of square-wave voltammetry. The performance of the system was assessed by analyzing samples of potassium ferrocyanide, caffeic acid and vanillic acid. Detection limits were at the nmol level; calibration graphs were rectilinear for, e.g., 100 µM vanillic acid.
Voltammetry
Electrode
Single bead string reactor
Glass beads