Contact Info
Stuart Chalk, Ph.D.
Department of Chemistry
University of North Florida
Phone: 1-904-620-1938
Fax: 1-904-620-3535
Email: schalk@unf.edu
Website: @unf
1,3-Dichloropropene
- IUPAC Name: (E)-1,3-dichloroprop-1-ene
- Molecular Formula: C3H4Cl2
- CAS Registry Number: 542-75-6
- InChI: InChI=1S/C3H4Cl2/c4-2-1-3-5/h1-2H,3H2
- InChI Key: UOORRWUZONOOLO-OWOJBTEDSA-N
Citations 1
"Derivatization Of Alkyl Halides, Acid Chlorides And Other Electrophiles With Polymer-immobilized 8-amino-2-naphthoxide"
J. Chromatogr. Sci.
1988 Volume 26, Issue 10 Pages 501-512
Colgan, S.T.;Krull, I.S.;Dorschel, C.;Bidlingmeyer, B.A.
Abstract:
Details are given for the normal- or reversed-phase HPLC determination of the cited compounds, with isocratic or gradient elution and UV, fluorimetric or amperometric detection. The 8-amino-2-naphthoxide was immobilized on AG1-X8 resin (Cl- form; Bio-Rad), which was packed into a column (3.3 cm x 3.9 mm) for use in pre- or post-analytical column derivatization. The acid chlorides react fast enough to allow online derivatization. Detection limits were in the sub-ppb range. The method was applied in the determination of cis- and trans-1,3-dichloropropene in water.
Water
HPLC
Amperometry
Fluorescence
Spectrophotometry
Immobilized reagent
Post-column derivatization
PPB